A new method for preparing powders for transmission electron microscopy examination

A. Montone, M. Vittori Antisari

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Abstract

In this paper we describe a novel method to prepare powder specimens for transmission electron microscopy examination. The powder samples are embedded in a metallic matrix by a route based on the plastic flow of a soft metal, using a small laboratory type hand driven hydraulic press. The resulting composites are processed with the conventional procedure based on grinding polishing and ion beam milling. The resulting TEM specimens have a self-supporting structure, good thermal and electrical conductivity while showing a well-polished surface resulting from the ion milling process. The method can be applied to a large variety of samples with sufficiently strong mechanical properties; a few examples are reported. The limits, mainly due to the mechanical toughness of the powder, are discussed. © 2003 Elsevier Science Ltd. All rights reserved.
Original languageEnglish
Pages (from-to)79 - 83
Number of pages5
JournalMicron
Volume34
Issue number2
DOIs
Publication statusPublished - 2003
Externally publishedYes

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All Science Journal Classification (ASJC) codes

  • Structural Biology
  • Cell Biology

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