The introduction of hydrogen into a metal during electrolysis of water involves primarily the metallic surface. The effect of surface morphology on electrochemical reaction kinetics is well described in the literature  therefore it seems to be reasonable to assume that the surface morphology of the cathodes could play a role in the electrochemical metal-hydride formation. Actually, a wide variety of surface features and profiles have been observed in the Pd cathodes typically employed in excess heat production experiments. These features are noted in both the as-prepared samples and the electrolyzed ones. In order to establish a correlation between the occurrence of a particular surface morphology and calorimetric results, it is necessary to identify a useful metric with which to describe and compare the different surface morphologies. In this work an approach based on Atomic Force Microscopy (AFM) has been investigated. The method is oriented toward the identification of parameters suitable for a pre-screening of the materials.
|Publication status||Published - 2008|
|Event||14th International Conference on Condensed Matter Nuclear Science and the 14th International Conference on Cold Fusion, ICCF-14 - , United States|
Duration: 1 Jan 2008 → …
|Conference||14th International Conference on Condensed Matter Nuclear Science and the 14th International Conference on Cold Fusion, ICCF-14|
|Period||1/1/08 → …|
All Science Journal Classification (ASJC) codes
- Nuclear Energy and Engineering
- Condensed Matter Physics
- Nuclear and High Energy Physics
- Atomic and Molecular Physics, and Optics
Sarto, F., Castagna, E., Sansovini, M., Lecci, S., Violante, V., Knies, D. L., & Grabowski, K. S. (2008). Electrode surface morphology characterization by atomic force microscopy. Paper presented at 14th International Conference on Condensed Matter Nuclear Science and the 14th International Conference on Cold Fusion, ICCF-14, United States.