Ligand mediated synthesis of AgInSe

Nadica D. Abazović, Mirjana I. Čomor, Miodrag N. Mitrić, Emanuela Piscopiello, Tamara Radetić, Ivana A. Janković, Jovan M. Nedeljković

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Abstract

Nanosized AgInSe2particles (d ∼ 7-25 nm) were synthesized using colloidal chemistry method at 270 °C. As solvents/surface ligands 1-octadecene, trioctylphosphine, and oleylamine were used. It was shown that choice of ligand has crucial impact not only on final crystal phase of nanoparticles, but also at mechanism of crystal growth. X-ray diffraction and TEM/HRTEM techniques were used to identify obtained crystal phases and to measure average size and shape of nanoparticles. UV/Vis data were used to estimate band-gap energies of obtained samples. It was shown that presented routes can provide synthesis of nanoparticles with desired crystal phase (tetragonal and/or orthorhombic), with band-gap energies in the range from 1.25 to 1.53 eV. © Springer Science+Business Media B.V. 2012.
Original languageEnglish
Article number810
Pages (from-to)-
JournalJournal of Nanoparticle Research
Volume14
Issue number4
DOIs
Publication statusPublished - 2012
Externally publishedYes

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All Science Journal Classification (ASJC) codes

  • Bioengineering
  • Atomic and Molecular Physics, and Optics
  • Chemistry(all)
  • Modelling and Simulation
  • Materials Science(all)
  • Condensed Matter Physics

Cite this

Abazović, N. D., Čomor, M. I., Mitrić, M. N., Piscopiello, E., Radetić, T., Janković, I. A., & Nedeljković, J. M. (2012). Ligand mediated synthesis of AgInSe. Journal of Nanoparticle Research, 14(4), -. [810]. https://doi.org/10.1007/s11051-012-0810-z