An original dissolution method for irradiated Li2TiO3in aqueous H2O2was developed. One could easily obtain fine Li2TiO3powders from the solution through drying and calcination. Li2TiO3pebbles (size ∼0.6 mm, above 90% TD) were obtained from the 'reprocessed' powders. These solutions were also suitable for the formation of a sol emulsion in 2-ethyl-hexanol-1, from which gelled microspheres of lithium titanate could be obtained. Locally prepared Li2TiO3reprocessed and supplied pebble batches were tested for tritium release by temperature programmed desorption (TPD) methods in He + 0.1%H2(R-gas) after their short irradiations in a thermal neutron flux. The relative TPD data were compared. A qualitative correlation was developed between peak characteristics and pebble microstructure. © 2001 Elsevier Science B.V.
All Science Journal Classification (ASJC) codes
- Electronic, Optical and Magnetic Materials
Alvani, C., Carconi, P. L., Casadio, S., Contini, V., Dibartolomeo, A., Pierdominici, F., ... Nannetti, C. A. (2001). Lithium titanate pebbles reprocessing by wet chemistry. Journal of Nuclear Materials, 289(3), 303 - 307. https://doi.org/10.1016/S0022-3115(01)00424-X